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P r o d u c t i o n   E q u i p m e n t

1

  • Synthesis on the basis of acetylene in liquid ammonia and on heterogeneous catalysts.
    • Temperature: -20 - +200 .
    • Pressure: upto 130 atm.
    • Capacity of periodic reactors (material): 5 l (stainless steel) and 50 l (stainless steel).
    Continuous reactors (stainless steel) output 50-100 ml/hour.

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    2
  • Hydrogenation on heterogeneous catalysts in stationary and continuous conditions.
    • Periodic reactors: 0,5 l (130 atm, stainless steel), 5 l (5 atm, stainless steel), 2*10 l (30 atm, stainless steel).
    • Temperature: till 220 .
    • Continuous reactors (stainless steel) output 50-200 ml/hour.
    • Pressure: till 400 atm.
    • Temperature: till 600 .
    • Volume of catalyst: till 50 ml.

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    3
  • Plants for preparation of catalysts.
    • Standard stirred apparatus for precipitated catalysts: 30 l (steel-enamel), 50 l (steel-enamel), 100 l (stainless steel), 250 l (cast iron-enamel), 5000 l (cast iron-enamel).
    • Nutsch filters, drying cabinets, impregnating drum, jaw crusher, roll mills, sieve series, mixers, ball mills, extrusion machine, tabletting machine. Muffle furnace for catalysts on the basis alloys, temperature 1800-2000 .
    • Distilling apparatus for water with output 20 l/hour.

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    4
  • Plant for purolysis of organic compounds in stream of inert gas or overheated steam in vacuum (down to 30 mm Hg).
    • Temperature: up to 500 .

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    5
  • Apparatus for fine organic synthesis.
    • Temperature: -50 - +220 .
    • Stirred reactors with explosion proof drives and jackets. 100 l (steel-enamel), 100 l (stainless steel), 2*60 l (steel- enamel), 50 l (stainless steel), 30 l (steel-enamel), 2*30 l (stainless steel), 2*30 l (stainless steel), 25 l (steel-enamel), 15 l (stainless steel) (working temperature till 270 ).
    • Autoclaves with magnetic drives 5 l (stainless steel), pressure 20 atm, 5 l (stainless steel), pressure 5 atm.
    • Reactors from glass @SIMAX@, 60 l, 50 l, 2*30 l.
    • Apparatus for periodic extraction 2*50 l (stainless steel), 2*25 l (stainless steel).
    • Six film rotating evaporators with 10 l flasks, working temperature till 220 , vacuum 3-5 mm Hg.
    • Distillation apparatus, working in high vacuum (10 -10 mm Hg).
    • Temperature: till 220
    • Output: 20 g/hour.
    • Nutsch and pressure filters.

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    6
  • Plants for recovery and refining of final products.
    • Plants of rectification (stainless steel) - still 100 l (stainless steel), efficiency 2-3 theoretical plates, output 4-5 l/hour.
    • Two columns of precise rectification (azeotropic and extractive).
    • Stills 50 l (stainless steel), efficiency 7 and 12 theoretical plates, output 1,5-3 l/hour.
    • Three glass columns of precise and superprecise rectification.
    • Stills 6 l (glass), efficiency 15-40 theoretical plates, output 30-50 ml/hour.
    • Columns of continuous extraction (glass):
      • packed column, efficiency 6 theoretical stages of separation;
      • sieve-tray column, efficiency 6 theoretical stages of separation.
    • Output on both phases 2-3 l/hour.

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