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T y p i c a l   P r o c e s s e s

Following chemical processes are developed for small industry
to produce 100 g - 10 Kg of chemical reagents:

1. Favorsky reaction (10-30 atm):
products from this reaction		  

1. FAVORSKY REACTION (10-30 atm)

2. Carol reaction (20-40 atm, H2/Pd, yield 85-95%):
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2. CAROL REACTION (20-40 atm, H2/Pd, yield 85-95%)

3. Selective hydrogenation: triple bond to double bond (20-40 atm, H2/Pd, selectivity 97-99%, conversion 90-95%):
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3. SELECTIVE HYDROGENATION: triple bond to double bond (20-40 atm, H2/Pd, selectivity 97-99%, conversion 90-95%)

4. Hydrogenetiona of aromatic nitrogroup (H2/Pd/C,20-40 atm; yeild 90-95%, R=Ar, Het):
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4. HYDROGENETIONA of AROMATIC NITROGROUP (H2/Pd/C,20-40 atm; yeild 90-95%, R=Ar, Het)

5. Hydrogenation of nitiriles (H2/Cat, 20 atm, yeild 92%):
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5.HYDROGENATION of NITIRILES (H2/Cat, 20 atm, yeild 92%)

6. Ammonia addition to activated double bond (NH4OH-H2O, 20 atm, yield 85-90%):
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6. AMMONIA ADDITION TO ACTIVATED DOUBLE BOND (NH4OH-H2O, 20 atm, yield 85-90%)

7. Methoxylation of olefines (ROH, Ion-exchange resin, yield 95%):
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7. METHOXYLATION of OLEFINES (ROH, Ion-exchange resin, yield 95%)

8. Mild electrooxidation of primary hydroxyl into aldehide (Cat/Br-, yield 90%):
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8.MILD ELECTROOXIDATION of PRIMARY HYDROXYL into ALDEHIDE (Cat/Br-, yield 90%)

9. Oxidative coupling of propargyl alcohols (Cu+, O2; yield 87%):
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9. OXIDATIVE COUPLING of PROPARGYL ALCOHOLS (Cu+, O2; yield 87%)

10. Cyclocarbonates from propargul alcohols ( CO2, 20-100 atm; yeild 95%):
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10. CYCLOCARBONATES from PROPARGUL ALCOHOLS ( CO2, 20-100 atm; yeild 95%)

11. Cyclocarbonates from epoxides ( CO2, 20-100 atm; yield 95%):
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11. CYCLOCARBONATES from EPOXIDES ( CO2, 20-100 atm; yield 95%)

12. Synthesis of yuvenile hormones (yield 87%):
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12.SYNTHESIS of YUVENILE HORMONES(yield 87%)

13. Acid chloroanhydrides from acids and thionyl chlorides (SOCl2, Cat:DMF; yield 93%):
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13. ACID CHLOROANHYDRIDES from ACIDS and THIONYL CHLORIDES (SOCl2, Cat:DMF; yield 93%)

14. Malondinitrile condensation with triethylorthoformate (Cat: Ac2O; yield 95%):
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14. MALONDINITRILE CONDENSATION with TRIETHYLORTHOFORMATE (Cat: Ac2O; yield 95%)

15. Nitroacetyl ester condensation with triethylorthoformate (Cat: Ac2O; yeild 90%):
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15. MALONDINITRILE CONDENSATION with TRIETHYLORTHOFORMATE (Cat: Ac2O; yeild 90%)

16. Nitration of nitroacetic ester in two-phase system (yield 90-95%):
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16. NITRATION of NITROACETIC ESTER in TWO-PHASE SYSTEM (yield 90-95%)

17. Amino to nitrogroup transformation for heterocycles (HNO2, yield 80-90%):
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17. AMINO to NITROGROUP TRANSFORMATION for HETEROCYCLES(HNO2, yield 80-90%)

18. N-Alkylation of 5-memberd nitrogen heterocycles by bromoketones (yoeld 80-90%):
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18. N-ALKYLATION of 5-MEMBERD NITROGEN HETEROCYCLES by BROMOKETONES (yoeld 80-90%)

19. Synthesis of monobromoacetone in two-phase system (Br2,KClO3,C4H4Cl2/H2O; yield 95%):
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19. SYNTHESIS of MONOBROMOACETONE in TWO-PHASE SYSTEM(Br2,KClO3,C4H4Cl2/H2O; yield 95%

20. One-step synthesis of 3,4-diamino-1,2,5-oxadiazole:
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20. ONE-STEP SYNTHESIS of 3,4-DIAMINO-1,2,5-OXADIAZOLE

21. Pyrolysis of cellulose into unhydrosugars (400 grad, vapor, vacuum 20 mmHg, Cat):
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21. PYROLYSIS of CELLULOSE into UNHYDROSUGARS (400 grad, vapor, vacuum 20 mmHg, Cat)

22. Oxydation of metyl in aromatic compounds:
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22. OXYDATION of METYL in AROMATIC compounds

23. One-step synthesis of 1-substituted tetrazoles:
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23. ONE-STEP SYNTHESIS of 1-SUBSTITUTED TETRAZOLES

24. Synthesis of trifluorobenzoic fluoroanhydrate in liqiud HF:
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24. Synthesis of trifluorobenzoic fluoroanhydrate in liqiud HF

25. Trifluoromethylation of p-nitrophenol:
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25. TRIFLUOROMETHYLATION OF P-NITROPHENOL

26. Catalyst for chiral aminoacid synthesis:
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26. CATALYST FOR CHIRAL AMINOACID SYNTHESIS

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